ANX-PR/CL/001-01 LEARNING GUIDE - Grado en Ingeniería ...
←
→
Transcripción del contenido de la página
Si su navegador no muestra la página correctamente, lea el contenido de la página a continuación
COORDINATION PROCESS OF
E.T.S. de Ingenieros de
LEARNING ACTIVITIES Caminos, Canales y Puertos
PR/CL/001
ANX-PR/CL/001-01
LEARNING GUIDE
SUBJECT
43000314 - Structural Characterization Of Materials I: Microscopy And Diffractometry
DEGREE PROGRAMME
04AF - Master Universitario En Ingenieria De Materiales
ACADEMIC YEAR & SEMESTER
2021/22 - Semester 1PR/CL/001
ANX-PR/CL/001-01 E.T.S. de Ingenieros de
COORDINATION PROCESS OF
LEARNING GUIDE Caminos, Canales y
LEARNING ACTIVITIES
Puertos
Index
Learning guide
1. Description...............................................................................................................................................................1
2. Faculty.....................................................................................................................................................................1
3. Prior knowledge recommended to take the subject..................................................................................................2
4. Skills and learning outcomes ...................................................................................................................................3
5. Brief description of the subject and syllabus.............................................................................................................5
6. Schedule..................................................................................................................................................................7
7. Activities and assessment criteria...........................................................................................................................10
8. Teaching resources.................................................................................................................................................12
9. Other information....................................................................................................................................................13PR/CL/001
ANX-PR/CL/001-01 E.T.S. de Ingenieros de
COORDINATION PROCESS OF
LEARNING GUIDE Caminos, Canales y
LEARNING ACTIVITIES
Puertos
1. Description
1.1. Subject details
43000314 - Structural Characterization Of Materials I: Microscopy And
Name of the subject
Diffractometry
No of credits 5 ECTS
Type Compulsory
Academic year ot the
First year
programme
Semester of tuition Semester 1
Tuition period September-January
Tuition languages English
Degree programme 04AF - Master Universitario en Ingenieria de Materiales
04 - Escuela Tecnica Superior De Ingenieros De Caminos, Canales Y
Centre
Puertos
Academic year 2021-22
2. Faculty
2.1. Faculty members with subject teaching role
Name and surname Office/Room Email Tutoring hours *
M - 11:00 - 12:00
Marta Clement Lorenzo
B-307 marta.clement@upm.es Appointments by
(Subject coordinator)
email
W - 11:00 - 12:00
Jimena Olivares Roza B-307 jimena.olivares@upm.es Appointments by
email
GA_04AF_43000314 Structural Characterization Of Materials I: Microscopy And Diffractometry Page 1 of 14
1S_2021-22 Master Universitario En Ingenieria De MaterialesPR/CL/001
ANX-PR/CL/001-01 E.T.S. de Ingenieros de
COORDINATION PROCESS OF
LEARNING GUIDE Caminos, Canales y
LEARNING ACTIVITIES
Puertos
M - 12:00 - 13:00
Jesus Sangrador Garcia B-308 jesus.sangrador@upm.es Appointments by
email
* The tutoring schedule is indicative and subject to possible changes. Please check tutoring times with the faculty
member in charge.
2.3. External faculty
Name and surname Email Institution
Luisa Ruiz Gonzalez luisarg@quim.ucm.es UCM
3. Prior knowledge recommended to take the subject
3.1. Recommended (passed) subjects
The subject - recommended (passed), are not defined.
3.2. Other recommended learning outcomes
- Structure of materials: Crystallography
- Mechanical properties of Materials
- Quantum Physics
- Electricity and Magnetism
- Instrumentation
GA_04AF_43000314 Structural Characterization Of Materials I: Microscopy And Diffractometry Page 2 of 14
1S_2021-22 Master Universitario En Ingenieria De MaterialesPR/CL/001
ANX-PR/CL/001-01 E.T.S. de Ingenieros de
COORDINATION PROCESS OF
LEARNING GUIDE Caminos, Canales y
LEARNING ACTIVITIES
Puertos
4. Skills and learning outcomes *
4.1. Skills to be learned
CB10 - Que los estudiantes posean las habilidades de aprendizaje que les permitan continuar estudiando de un
modo que habrá de ser en gran medida autodirigido o autónomo
CB6 - Poseer y comprender conocimientos que aporten una base u oportunidad de ser originales en el desarrollo
y/o aplicación de ideas, a menudo en un contexto de investigación
CB7 - Que los estudiantes sepan aplicar los conocimientos adquiridos y su capacidad de resolución de problemas
en entornos nuevos o poco conocidos dentro de contextos más amplios (o multidisciplinares) relacionados con su
área de estudio
CB9 - Que los estudiantes sepan comunicar sus conclusiones ¿y los conocimientos y razones últimas que las
sustentan¿ a públicos especializados y no especializados de un modo claro y sin ambigüedades
CE 1 - Conocer, comprender y saber aplicar los fundamentos científicos del comportamiento físico y químico de los
materiales para saber relacionar causalmente sus propiedades fundamentales físicas y químicas con su
comportamiento y el de los productos con ellos realizados.
CE 4 - Conocer, comprender, identificar y saber determinar la composición y estructura de los diversos tipos de
materiales, conociendo y siendo capaz de aplicar y utilizar las técnicas y los equipos experimentales de
caracterización y análisis micro y macroestructural, mecánico, eléctrico, magnético y óptico de los materiales.
CE 5 - Ser capaz de entender, aprender, actualizar autónomamente y aplicar nuevos conocimientos, modelos y
técnicas experimentales y numéricas en relación con la composición y estructura de los materiales, su
caracterización física y química, sus procesos de fabricación, su utilización y aplicación científica y tecnológica, y
su reciclado, reutilización y eliminación.
CG1 - Uso de la lengua inglesa para comunicar conocimientos, ideas y argumentos de manera clara, rigurosa y
convincente.
CG3 - Creatividad para pensar o resolver de forma nueva y original situaciones o problemas en el ámbito de la
ciencia, la ingeniería y la tecnología.
CG5 - Gestión de la información que permita buscar, seleccionar y analizar con habilidad y eficacia la información
más relevante procedente de diversas fuentes analógicas y digitales
GA_04AF_43000314 Structural Characterization Of Materials I: Microscopy And Diffractometry Page 3 of 14
1S_2021-22 Master Universitario En Ingenieria De MaterialesPR/CL/001
ANX-PR/CL/001-01 E.T.S. de Ingenieros de
COORDINATION PROCESS OF
LEARNING GUIDE Caminos, Canales y
LEARNING ACTIVITIES
Puertos
4.2. Learning outcomes
RA8 - RD.3:Que los estudiantes sepan comunicar sus conclusiones (y los conocimientos y razones últimas que las
sustentan) a públicos especializados y no especializados de un modo claro y sin ambigüedades;
RA36 - Capacity for interpreting scientific results
RA38 - Conocer y saber manejar los conceptos que definen la estructura de los materiales cristalinos y amorfos,
de los materiales metálicos, cerámicos, polímeros y biológicos y sus principios de organización.
RA79 - Ser capaz de elegir la técnica de caracterización de la estructura de los materiales más adecuada a los
problemas planteados
RA76 - Saber redactar informes técnicos
RA5 - RD0. Poseer y comprender conocimientos que aporten una base u oportunidad de ser originales en el
desarrollo y/o aplicación de ideas, a menudo en un contexto de investigación
RA58 - Utilizar con soltura la comunicación oral y escrita en lengua española e inglesa.
RA40 - Conocer y saber utilizar las técnicas experimentales más avanzadas para determinar la estructura de los
materiales desde su nivel atómico al macroscópico. Saber aplicarlas para controlar y cambiar la conformación de
los materiales.
RA80 - Saber interpretar las medidas obtenidas de tecnicas de caracterización estructural de los materiales
RA23 - Conocer, comprender y saber aplicar las bases de la ciencia y del método científico
RA18 - Conocer, comprender y saber aplicar los fundamentos científicos del comportamiento de los materiales y la
interrelación entre su estructura, propiedades, procesado y aplicaciones
RA2 - Saber comunicar conocimientos, procedimientos, resultados o técnicas relacionadas con el comportamiento
y el uso de materiales
RA32 - Conocer, comprender y saber aplicar los fundamentos científicos del comportamiento de los materiales
RA1 - Ser capaz de aprender y actualizar autónomamente nuevos conocimientos y técnicas
RA43 - Utilizar con soltura la comunicación oral y escrita en lengua española e inglesa
* The Learning Guides should reflect the Skills and Learning Outcomes in the same way as indicated in the Degree
Verification Memory. For this reason, they have not been translated into English and appear in Spanish.
GA_04AF_43000314 Structural Characterization Of Materials I: Microscopy And Diffractometry Page 4 of 14
1S_2021-22 Master Universitario En Ingenieria De MaterialesPR/CL/001
ANX-PR/CL/001-01 E.T.S. de Ingenieros de
COORDINATION PROCESS OF
LEARNING GUIDE Caminos, Canales y
LEARNING ACTIVITIES
Puertos
5. Brief description of the subject and syllabus
5.1. Brief description of the subject
This course aims at the advanced understanding of the operation principles of various characterization techniques,
based on microscopies (optical microscopy, scanning electron microscopy, transmission electron microscopy
electron, atomic froce microscopy, scanning tunneling microscopy) and diffractometries (X-ray diffraction, electron
diffraction).
The course addresses the basics of the techniques, the underlying physics, the instrumental aspects, the practical
use and the benefits and problems related to their application in materials science and microelectronics.
Combined with practical work at microscopes and diffractometers, the student will be able to process and interpret
images and data. Completion of this course will give the participant a working knowledge on how microscopy
techniques are applied in materials research and development. At the end of the course, it is expected that the
student can apply the appropriate technique to a given material to be characterized and that he/she is able to
interpret data and to extract valuable information.
Objectives
1) To learn the fundamentals of the main techniques
2) To become familiar with instrumentation and experimental set-ups
3) To learn how to analyze experimental data
4) To be able to select the most appropriate characterization technique
GA_04AF_43000314 Structural Characterization Of Materials I: Microscopy And Diffractometry Page 5 of 14
1S_2021-22 Master Universitario En Ingenieria De MaterialesPR/CL/001
ANX-PR/CL/001-01 E.T.S. de Ingenieros de
COORDINATION PROCESS OF
LEARNING GUIDE Caminos, Canales y
LEARNING ACTIVITIES
Puertos
5.2. Syllabus
1. Introduction
2. Optical Microscopy
3. Profilometry
4. Scanning tunneling microscopy
5. Atomic force microscopy
6. X-ray diffraction
7. Electron diffraction
8. Transmission electron microscopy
9. Scanning electron microscopy
GA_04AF_43000314 Structural Characterization Of Materials I: Microscopy And Diffractometry Page 6 of 14
1S_2021-22 Master Universitario En Ingenieria De MaterialesPR/CL/001
ANX-PR/CL/001-01 E.T.S. de Ingenieros de
COORDINATION PROCESS OF
LEARNING GUIDE Caminos, Canales y
LEARNING ACTIVITIES
Puertos
6. Schedule
6.1. Subject schedule*
Week Face-to-face classroom activities Face-to-face laboratory activities Distant / On-line Assessment activities
Introduction to te course. Timetable,
student groups, assessment and topics.
1
Duration: 03:00
Lecture
Optical microscopy
Duration: 01:30
Lecture
2
Profilometry
Duration: 01:30
Lecture
Scanning Electron Microscopy (SEM) Multiple choice exam 1 (OM-PR)
Duration: 02:45 Online test
Lecture Continuous assessment
Presential
Duration: 00:15
3
Deliverable 1: Profilometry and Light
Microscopy
Individual work
Continuous assessment
Not Presential
Duration: 00:00
Scanning tunnel microscopy Multiple choice exam 2 (SEM)
Duration: 01:20 Online test
4 Lecture Continuous assessment
Presential
Duration: 00:15
Atomic force microscopy Multiple choice exam 3 (STM)
Duration: 01:20 Online test
Lecture Continuous assessment
Presential
Duration: 00:15
5
Deliverable 2: AFM and STM
Individual work
Continuous assessment
Not Presential
Duration: 00:00
Laboratory Session G1-G6
6 Duration: 03:00
Laboratory assignments
GA_04AF_43000314 Structural Characterization Of Materials I: Microscopy And Diffractometry Page 7 of 14
1S_2021-22 Master Universitario En Ingenieria De MaterialesPR/CL/001
ANX-PR/CL/001-01 E.T.S. de Ingenieros de
COORDINATION PROCESS OF
LEARNING GUIDE Caminos, Canales y
LEARNING ACTIVITIES
Puertos
Laboratory Session G1-G6
7 Duration: 03:00
Laboratory assignments
Laboratory Session G1-G6
8 Duration: 03:00
Laboratory assignments
Oral Presentations Multiple choice exam 4 (AFM)
Duration: 01:00 Online test
Cooperative activities Continuous assessment
Presential
X-Ray Diffraction Duration: 00:15
9 Duration: 02:00
Lecture Deliverable 3: AFM data handling
Individual work
Continuous assessment
Not Presential
Duration: 00:00
Oral Presentations Multiple choice exam 5 (Lab activity)
Duration: 01:00 Online test
Cooperative activities Continuous assessment
10 Presential
X-Ray Diffraction Duration: 00:15
Duration: 02:00
Lecture
Oral Presentations X-Ray Diffraction. Visit to UCM facilities Multiple choice exam 6 (XRD-I)
Duration: 01:00 (morning session) Online test
Cooperative activities Duration: 04:00 Continuous assessment
11 Laboratory assignments Presential
X-Ray Diffraction Duration: 00:15
Duration: 02:00
Lecture
Oral Presentations X-Ray Diffraction. Data handling Multiple choice exam 7 (XRD-II)
Duration: 01:00 Duration: 03:00 Online test
Cooperative activities Laboratory assignments Continuous assessment
Presential
Duration: 00:15
12
Deliverable 4: XRD data handling
Individual work
Continuous assessment
Not Presential
Duration: 00:00
Transmission electron microscopy and Oral presentation
related techniques Individual presentation
Duration: 02:00 Continuous assessment
Lecture Not Presential
13
Duration: 00:00
Oral Presentations
Duration: 01:00
Cooperative activities
Laboratory Session: Visit to TEM Multiple choice exam 8 (TEM)
facilities at UCM Online test
14 Duration: 04:00 Continuous assessment
Laboratory assignments Presential
Duration: 00:15
GA_04AF_43000314 Structural Characterization Of Materials I: Microscopy And Diffractometry Page 8 of 14
1S_2021-22 Master Universitario En Ingenieria De MaterialesPR/CL/001
ANX-PR/CL/001-01 E.T.S. de Ingenieros de
COORDINATION PROCESS OF
LEARNING GUIDE Caminos, Canales y
LEARNING ACTIVITIES
Puertos
Continuos assessment exam
Written test
15 Continuous assessment
Presential
Duration: 02:00
Final exam will consist in a multiple
choice test dealing with all the
theoretical subjects tackled during the
course. 60% 4 Deliverables: 20% Oral
16 presentation: 20%
Written test
Final examination
Presential
Duration: 02:00
17
Depending on the programme study plan, total values will be calculated according to the ECTS credit unit as 26/27
hours of student face-to-face contact and independent study time.
* The schedule is based on an a priori planning of the subject; it might be modified during the academic year,
especially considering the COVID19 evolution.
GA_04AF_43000314 Structural Characterization Of Materials I: Microscopy And Diffractometry Page 9 of 14
1S_2021-22 Master Universitario En Ingenieria De MaterialesPR/CL/001
ANX-PR/CL/001-01 E.T.S. de Ingenieros de
COORDINATION PROCESS OF
LEARNING GUIDE Caminos, Canales y
LEARNING ACTIVITIES
Puertos
7. Activities and assessment criteria
7.1. Assessment activities
7.1.1. Continuous assessment
Minimum
Week Description Modality Type Duration Weight Evaluated skills
grade
CE 5
3 Multiple choice exam 1 (OM-PR) Online test Face-to-face 00:15 1.88% 4 / 10
CE 4
CE 5
Deliverable 1: Profilometry and Individual CE 4
3 No Presential 00:00 3% 4 / 10
Light Microscopy work CB7
CE 1
CE 4
4 Multiple choice exam 2 (SEM) Online test Face-to-face 00:15 1.88% 4 / 10 CE 1
CE 5
5 Multiple choice exam 3 (STM) Online test Face-to-face 00:15 1.88% 4 / 10
CB7
Deliverable 2: AFM and Individual CE 1
5 No Presential 00:00 3% / 10
STM work CE 5
CE 4
9 Multiple choice exam 4 (AFM) Online test Face-to-face 00:15 1.88% 4 / 10
CE 5
Individual
9 Deliverable 3: AFM data handling No Presential 00:00 3% / 10 CE 4
work
CE 1
CE 5
Multiple choice exam 5 (Lab
10 Online test Face-to-face 00:15 1.87% 4 / 10 CE 4
activity)
CE 1
11 Multiple choice exam 6 (XRD-I) Online test Face-to-face 00:15 1.87% 4 / 10
12 Multiple choice exam 7 (XRD-II) Online test Face-to-face 00:15 1.87% 4 / 10
Individual
12 Deliverable 4: XRD data handling No Presential 00:00 6% / 10
work
Individual
13 Oral presentation No Presential 00:00 20% / 10
presentation
CE 1
14 Multiple choice exam 8 (TEM) Online test Face-to-face 00:15 1.87% 4 / 10 CE 5
CE 4
CG3
CB6
CE 5
CB10
CG1
15 Continuos assessment exam Written test Face-to-face 02:00 50% 4 / 10
CE 4
CB9
GA_04AF_43000314 Structural Characterization Of Materials I: Microscopy And Diffractometry Page 10 of 14
1S_2021-22 Master Universitario En Ingenieria De MaterialesPR/CL/001
ANX-PR/CL/001-01 E.T.S. de Ingenieros de
COORDINATION PROCESS OF
LEARNING GUIDE Caminos, Canales y
LEARNING ACTIVITIES
Puertos
CB7
CG5
CE 1
7.1.2. Final examination
Minimum
Week Description Modality Type Duration Weight Evaluated skills
grade
CG3
CB6
Final exam will consist in a multiple
CE 5
choice test dealing with all the
CB10
theoretical subjects tackled during
CG1
16 the course. 60% Written test Face-to-face 02:00 100% 5 / 10
CE 4
CB9
4 Deliverables: 20%
CB7
Oral presentation: 20%
CG5
CE 1
7.1.3. Referred (re-sit) examination
Minimum
Description Modality Type Duration Weight Evaluated skills
grade
Extraordinary exam will consist in a
multiple choice test dealing with all
the theoretical subjects tackled
Written test Face-to-face 02:00 100% 5 / 10
during the course. 60% 4
Deliverables: 20% Oral
presentation: 20%
GA_04AF_43000314 Structural Characterization Of Materials I: Microscopy And Diffractometry Page 11 of 14
1S_2021-22 Master Universitario En Ingenieria De MaterialesPR/CL/001
ANX-PR/CL/001-01 E.T.S. de Ingenieros de
COORDINATION PROCESS OF
LEARNING GUIDE Caminos, Canales y
LEARNING ACTIVITIES
Puertos
7.2. Assessment criteria
Continuous assessment:
Attendance to practical sessions (laboratory and simulation sessions) is mandatory. Non-attendance to a practical
session will be penalized with 0.5 points of the final mark.
Attendance to oral presentations is mandatory. Active participation in oral presentation (questions, remarks etc.)
will be rewarded with up to 1 extra point in the final mark.
8. Teaching resources
8.1. Teaching resources for the subject
Name Type Notes
http://mse.iastate.edu/microscopy/ho
Web resource
me.html
R. Haynes B.Met., Ph.D., C.Eng.,
F.I.M., M.Inst.P. "Optical Microscopy Bibliography
of Materials", Springer (1984)
P. Eaton and P. West "Atomic force
Bibliography
microscopy", Oxford Press (2010)
GA_04AF_43000314 Structural Characterization Of Materials I: Microscopy And Diffractometry Page 12 of 14
1S_2021-22 Master Universitario En Ingenieria De MaterialesPR/CL/001
ANX-PR/CL/001-01 E.T.S. de Ingenieros de
COORDINATION PROCESS OF
LEARNING GUIDE Caminos, Canales y
LEARNING ACTIVITIES
Puertos
http://www.mrl.ucsb.edu/mrl/centralfa
Web resource
cilities/xray/xray-basics/index.html
B.D. Cullity, "Elements of X-ray
Bibliography
diffraction"
B. K. Vainshtein, E. Feigl and J.A.
Spink, "Structure Analysis by
Bibliography
Electron Diffraction", Pergamon
Press (1964)
L. Reimer, H. Kohl, "Transmission
Electron Microscopy: Physics of
Bibliography
Image Formation" Springer Verlag
(2008)
L. Reimer, "Scanning electron
microscopy: physics of image
Bibliography
formation and microanalysis",
Springer-Verlag (1985/1998).
Research laboratories of GMME- Clean room with several characterization
Equipment
UPM techniques
CAI X-ray diffraction Equipment X-Ray diffraction service at UCM
Electron microscopy lab Equipment Electron microscopy seervice at UCM
SRIB Equipment Scanning reactive ion beam lab at CIEMAT
9. Other information
9.1. Other information about the subject
This course invests a significant time and effort to demonstration activities. Several external laboratories will
be visited to see and learn practical aspects of the different characterization techniques.
The schedule is based on an a priori planning of the subject; it might be modified during the academic year,
especially considering the COVID19 evolution. Both teaching and assessment activities may be turned into
on-line activities if required by the health situation.
Communication between students and lecturers will take place by email. The students are encouraged to
send an email to the coordinator or any specific lecturer for any concern related to the module. As far as
possible, the lecturers will answer with the least possible delay.
GA_04AF_43000314 Structural Characterization Of Materials I: Microscopy And Diffractometry Page 13 of 14
1S_2021-22 Master Universitario En Ingenieria De MaterialesPR/CL/001
ANX-PR/CL/001-01 E.T.S. de Ingenieros de
COORDINATION PROCESS OF
LEARNING GUIDE Caminos, Canales y
LEARNING ACTIVITIES
Puertos
Tutorials will take place either face-to-face or through Skype if face-to-face activities are not allowed.
On-line teaching (if necessary) will take place through Business Skype or Teams platforms.
Sustainable Development Goals
Although the topics tackled in the module do not directly address any specific SDG, students from different
countries are encouraged to work together in groups, according to SDG-17. In addition, we also
recommend them to choose topics for their oral presentations dealing with the characterization of materials
that suffer some kind of degradation (climate changes, pollution, desertification) addressed by SDGs 13, 14
and 15.
GA_04AF_43000314 Structural Characterization Of Materials I: Microscopy And Diffractometry Page 14 of 14
1S_2021-22 Master Universitario En Ingenieria De Materiales
Powered by TCPDF (www.tcpdf.org)También puede leer
